Summary
A study was made of the problems encountered when the chromatogram of a sample being analyzed for PCB's via GLC cannot readily be compared to a particular Aroclor standard. The use of mixed Aroclor standards was proposed and a study made of the effect of mixed standards on the analytical results. It was found that the choice of a standard could alter the values by more than a factor of 2. In addition, the particular mixture used as a standard should be reported along with resulting values.
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References
ARMOUR, J.A. and BURKE, J.A., J. Ass. Offic. Anal. Chem.53, 761 (1970)
HANSEN, D.J.et al., Bull. Environ. Contam. Toxicol.6,113 (1971)
KOEMAN, J.H.et al., Nature221,1126 (1969)
MULHERN, B.et al., J. Ass. Offic. Anal. Chem.54, 548 (1971)
QUINBY, G.E. ed., Polychlorobiphenyls (PCB's) and Related Chlorophenyls: Effects on Environment, Vol. I, Bibliography 1881–1971, (1972), Oak Ridge National Laboratory, Oak Ridge,
Tennessee (Oak Ridge Order No. TIRC-1, ORNL-EIS-72-20)
REINERT, R.E., Pestic. Monit. J.3, 233 (1970)
REINERT, R.E. and SNYDER, D., Bull. Environ. Contam. Toxicol.6,385 (1971)
RISEBROUGH, R.W.et al., Nature220,1098 (1968)
RISEBROUGH, R.W.et al., Bull. Environ. Contam. Toxicol.4,192 (1969)
SKRENTNY, R.F., Bull. Environ. Contam. Toxicol.6, 409 (1971)
ZITKO, V., Bull. Environ. Contam. Toxicol.6,464 (1971a)
ZITKO, V., Bull. Environ. Contam. Toxicol.6,160 (1971b)
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Beezhold, F.L., Stout, V.F. The use and effect of mixed standards on the quantitation of polychlorinated biphenyls. Bull. Environ. Contam. Toxicol. 10, 10–15 (1973). https://doi.org/10.1007/BF01684748
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DOI: https://doi.org/10.1007/BF01684748