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Determination of Hymexazol in Cucumber and Soil Samples by Derivatization Using GC-FPD

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Abstract

A sensitive and effective analytical method for the determination of hymexazol in cucumber and soil samples by gas chromatography with a flame photometric detector was developed. This method was validated with fortified at three different levels of 0.2, 1.0 and 5.0 mg/kg. Average recoveries obtained from cucumber and soil samples at three fortified levels were 94.0%–107.8% with relative standard deviations (RSDs) of less than 11.4%. Limits of quantification (LOQ) in cucumber and soil were 0.2 mg/kg. The method was successfully applied to determine hymexazol in real samples of cucumber and soil under open fields.

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References

  • Argauer RJ (1969) Determination of residues of banol and other carbamate pesticides after hydrolysis and chloroacetylation. J Agric Food Chem 17:888–892

    Article  CAS  Google Scholar 

  • Butler LI, Madonough LM (1968) Mehods for the determination of residues of carbamate insecticides by elsetron-capture gas chromatography. J Agric Food Chem 16:403

    Article  CAS  Google Scholar 

  • Pilar V, Nerea A, Natalia C, Manuel HC (2008) Comparison of stir bar sorptive extraction and membrane-assisted solvent extraction for the ultra-performance liquid chromatographic determination of oxazole fungicide residues in wines and juices. J Chromatogr A 1194:178–183

    Article  Google Scholar 

  • Qian K, He S, Tang T, Shi TY, Li JQ, Cao YS (2011) A rapid liquid chromatography method for determination of glufosinate residue in maize after derivation. Food Chem 127:722–726

    Article  CAS  Google Scholar 

  • Tamura Y, Takano I, Kobayashi M, Tomizawa S, Tateishi Y, Sakai N, Ibe A, Nagayama T (2008) Determination of hymexazol in agricultural products by GC-NPD. J Food Hyg Soc Jpn 49(03):223–227

    Article  CAS  Google Scholar 

  • Zhang SQ, Cooper JF (1996) Adsorption, desorption, and degradation of three pesticides in different soils. Arch Environ Contam Toxicol 30:15–20

    Article  Google Scholar 

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Acknowledgments

This work was supported by grants from the Institute for the Control of Agrochemicals, Ministry of Agriculture of the People’s Republic of China.

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Authors and Affiliations

  1. Key Laboratory of Natural Pesticide and Chemical Biology, Ministry of Education, South China Agricultural University, Guangzhou, 510642, People’s Republic of China

    Dali Sun, Huochun Ye & Chenglan Liu

  2. State Key Laboratory of Integrated Management of Pest Insects and Rodents Institute of Zoology, Chinese Academy of Sciences, Beijing, 100101, People’s Republic of China

    Li Li, Wei Li & Yijun Wu

  3. Beijing Research Institute of Chemical Industry, SINOPEC, Beijing, 100013, People’s Republic of China

    Ran Ji

Authors
  1. Dali Sun
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  2. Li Li
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  3. Ran Ji
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  4. Wei Li
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  5. Huochun Ye
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  6. Yijun Wu
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  7. Chenglan Liu
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Correspondence to Chenglan Liu.

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Sun, D., Li, L., Ji, R. et al. Determination of Hymexazol in Cucumber and Soil Samples by Derivatization Using GC-FPD. Bull Environ Contam Toxicol 87, 653–656 (2011). https://doi.org/10.1007/s00128-011-0421-x

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  • DOI: https://doi.org/10.1007/s00128-011-0421-x

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