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X-Ray Photoelectron Spectroscopy of Nanodiamonds Obtained by Grinding and Detonation Synthesis

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Abstract

The initial composition and chemical state of nanopowder primary particles obtained by grinding natural diamond and detonation synthesis have been studied by X-ray photoelectron spectroscopy. It has been shown that the primary particles of both nanopowders contain mainly carbon and oxygen atoms. The signals from nitrogen, sulfur, chlorine, and metal atoms in the photoelectronic spectrum do not exceed the noise level. It has been discovered that the proportions of carbon atoms are ∼46.5 and ∼67.8% in the state of the sp3 hybridization, ∼26.8 and ∼17.4% in the state of the sp2-hybridization, and ∼26.7 and ∼14.7% in the composition of the oxygen-containing functional groups in the primary particles of the nanopowders obtained by detonation synthesis and by grinding natural diamond, respectively.

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REFERENCES

  1. P. P. Sharin, A. V. Sivtseva, and V. I. Popov, Tech. Phys. Lett. 46 (2), 145 (2020). https://doi.org/10.1134/S1063785020020133

    Article  ADS  Google Scholar 

  2. P. P. Sharin, A. V. Sivtseva, S. P. Yakovleva, M. M. Kopyrin, S. A. Kuzmin, V. I. Popov, and L.  A.  Nikiforov, Izv. Vyssh. Uchebn. Zaved., Porosh. Metallurg. Funktsion. Pokryt., No. 4, 55 (2019). https://doi.org/10.17073/1997-308X-2019-4-55-67

  3. I. I. Kulakova, Phys. Solid State 46 (4), 636 (2004). https://doi.org/10.1134/1.1711440

    Article  ADS  Google Scholar 

  4. V. I. Korepanov, H. Hamaguchi, E. Osawa, V. Ermolenkov, I. K. Lednev, B. J. M. Etzold, O. Levinson, B. Zousman, C. P. Epperla, and H.-C. Chang, Carbon 121, 322 (2017). https://doi.org/10.1016/j.carbon.2017.06.012

    Article  Google Scholar 

  5. A. L. Vereshchagin, Properties of Detonation Nanodiamonds (Altay Gos. Tekh. Univ., Biysk, 2003) [in Russian].

    Google Scholar 

  6. S. Stehlik, M. Varga, M. Ledinsky, V. Jrashek, A. Artemenko, H. Kozak, L. Ondic, V. Skakalova, G. Argentero, T. Pennycook, J. Meyer, A. Fejfar, A. Kromka, and B. Rezek, J. Phys. Chem. 119, 27708 (2015). https://doi.org/10.1021/acs.jpcc.5b05259

    Article  Google Scholar 

  7. D. E. Nikolichev, A. V. Boryakov, S. I. Surodin, and R. N. Kryukov, Analysis of Solid-State Heterogeneity by XPS. Training Manual (Nizhegorod. Gos. Univ., Nizhniy Novgorod, 2013) [in Russian].

    Google Scholar 

  8. Deep Cleaning Technology Ultrafine Diamonds. http://www.frpc.secna.ru/uda/propert.php.

  9. A. E. Aleksenskii, V. Yu. Osipov, A. Ya. Vul’, B. Ya. Ber, A. B. Smirnov, V. G. Melekhin, G. J. Adriaenssens, and K. Iakoubovskii, Phys. Solid State 43 (1), 145 (2001). https://doi.org/10.1134/1.1340200

    Article  ADS  Google Scholar 

  10. http://xpspeak.software.informer.com/4.1.

  11. C. Fang, Yu. Zhang, W. Shen, Sh. Sun, Zh. Zhang, L. Xue, and X. Jia, CrystEngComm 19, 5727 (2017).

    Article  Google Scholar 

  12. M. Qi, J. Xiao, Y. Cheng, Zh. Wang, A. Jiang, Y. Guo, and Z. Tao, AIP Adv. 7, 085012 (2017).

    Article  ADS  Google Scholar 

  13. A. V. Shvidchenko, A. N. Zhukov, A. T. Dideikin, M. V. Baidakova, M. S. Shestakov, V. V. Shnitov, and A. Ya. Vul’, Colloid J. 78 (2), 235 (2016). https://doi.org/10.1134/S1061933X16020149

    Article  Google Scholar 

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Authors and Affiliations

  1. Larionov Institute of Physical and Technical Problems of the North, Federal Research Center, Yakutsk Scientific Center, Siberian Branch, Russian Academy of Sciences, 677980, Yakutsk, Russia

    P. P. Sharin & A. V. Sivtseva

  2. Ammosov North Eastern Federal University, 677980, Yakutsk, Russia

    V. I. Popov

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  1. P. P. Sharin
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  2. A. V. Sivtseva
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  3. V. I. Popov
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Correspondence to P. P. Sharin.

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Translated by N. Petrov

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Sharin, P.P., Sivtseva, A.V. & Popov, V.I. X-Ray Photoelectron Spectroscopy of Nanodiamonds Obtained by Grinding and Detonation Synthesis. Tech. Phys. 66, 275–279 (2021). https://doi.org/10.1134/S1063784221020183

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  • DOI: https://doi.org/10.1134/S1063784221020183

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