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Synthesis and crystal structure of a Pb complex with ciprofloxacin

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Abstract

A hydrothermal reaction of ciprofloxacin with PbCl2 · 2H2O and Na2S yields a metal complex [Pb2(H-Cip)6S]Cl6 (I), which was characterized by elemental analysis, IR, and single crystal diffraction analyses. Complex I crystallizes in the rhombohedral system, space group \(R\bar 3c\), with lattice parameters a = 15.7800(7), c = 77.901(9) Å, V = 16799(2) Å3, Z = 12, ρcalcd = 1.646 mg/m3.

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Authors and Affiliations

  1. Key Laboratory of Theoretical Chemistry and Molecular Simulation of Ministry of Education, Hunan Provincial University Key Laboratory of QSAR/QSPR, School of Chemistry and Chemical Engineering, Hunan University of Science and Technology, Xiangtan, 411201, P.R. China

    L. C. Yu & H. M. Peng

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  1. L. C. Yu
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  2. H. M. Peng
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Correspondence to L. C. Yu.

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Yu, L.C., Peng, H.M. Synthesis and crystal structure of a Pb complex with ciprofloxacin. Russ J Coord Chem 38, 392–395 (2012). https://doi.org/10.1134/S1070328412060115

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  • DOI: https://doi.org/10.1134/S1070328412060115

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