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Synthesis and Structure of Fe-Fe3O4 Nanoparticles with “Core-Shell” Architecture Capsulated in a Graphite-Like Carbon Matrix

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Journal of Contemporary Physics (Armenian Academy of Sciences) Aims and scope

Abstract

Nanoparticles of iron (α-Fe) and iron oxide (Fe3O4) with a core-shell structure (α-Fe core, Fe3O4 shell) covered with additional graphite-like carbon layer have been synthesized. The samples were obtained by solid-phase pyrolysis of iron phthalocyanine (FePc) at a pyrolysis temperature of 1000°C, followed by annealing in an oxygen atmosphere at a temperature of 250°C. The composition, structure and morphology of the samples were investigated by transmission and scanning transmission electron microscopy with elemental mapping, synchrotron X-ray diffraction and Raman spectroscopy.

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Funding

This work was supported by a grant from the Russian-Armenian (Slavonic) University at the support of the Ministry of Education and Science of the Russian Federation. This work was also supported by a grant from the American National Science Foundation No. HRD-1547723.

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Authors and Affiliations

  1. Russian–Armenian University, Yerevan, Armenia

    A. T. Gyulasaryan, G. K. Chilingaryan & A. S. Manukyan

  2. Institute for Physical Research, NAS of Armenia, Ashtarak, Armenia

    A. T. Gyulasaryan, N. Sisakyan, G. K. Chilingaryan, E. G. Sharoyan & A. S. Manukyan

  3. California State University, Los Angeles, USA

    K. A. Castillo, O. O. Bernal & A. N. Kocharian

  4. Kurchatov National Research Center Institute, Moscow, Russia

    A. A. Veligzhanin

  5. Institute for Materials Research, State University Pennsylvania, Pennsylvania, USA

    J. L. Gray

Authors
  1. A. T. Gyulasaryan
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  2. K. A. Castillo
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  3. O. O. Bernal
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  4. A. N. Kocharian
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  5. N. Sisakyan
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  6. G. K. Chilingaryan
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  7. A. A. Veligzhanin
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  8. J. L. Gray
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  9. E. G. Sharoyan
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  10. A. S. Manukyan
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Corresponding author

Correspondence to A. N. Kocharian.

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The authors declare no conflict of interest.

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Translated by V.M. Aroutiounian

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Gyulasaryan, A.T., Castillo, K.A., Bernal, O.O. et al. Synthesis and Structure of Fe-Fe3O4 Nanoparticles with “Core-Shell” Architecture Capsulated in a Graphite-Like Carbon Matrix. J. Contemp. Phys. 56, 150–153 (2021). https://doi.org/10.3103/S1068337221020079

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  • DOI: https://doi.org/10.3103/S1068337221020079

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