Abstract
The effect of temperature on grinding-induced texture in tetragonal lead zirconate titanate (PZT) and lead titanate (PT) has been investigated using in situ x-ray diffraction (XRD) with an area detector. In contrast with previous results on electrical poling, mechanically-ground PT and soft PZT materials retain strong ferroelastic textures during thermal cycling, even after excursions to temperatures slightly above the Curie temperature. The relationship between the residual stresses in the surface region, caused by grinding, and those resulting from domain wall motion is elucidated by in situ texture measurements obtained during thermal cycling.
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W. Chang, A.H. King K.J. Bowman: Thermal effects on domain orientation of tetragonal piezoelectrics studied by in situ x-ray diffraction. Appl. Phys. Lett. 88, 242901 2006
K.J. Bowman: Texture from domain switching of tetragonal zirconias. J. Am. Ceram. Soc. 74(10), 2690 1991
A.V. Virkar R.L.K. Matsumoto: Ferroelastic domain switching as a toughening mechanism in tetragonal zirconia. J. Am. Ceram. Soc. 69(10), C224 1986
K. Mehta A.V. Virkar: Fracture mechanisms in ferroelectric-ferroelastic lead zirconate titanate (Zr:Ti=0.54:0.46) ceramics. J. Am. Ceram. Soc. 73(3), 567 1990
S. Cheng, I.K. Lloyd M. Kahn: Modification of surface texture by grinding and polishing lead zirconate titanate ceramics. J. Am. Ceram. Soc. 75(8), 2293 1992
B-S. Li, J-S. Cherng, K.J. Bowman I-W. Chen: Domain switching as a toughening mechanism in tetragonal zirconia. J. Am. Ceram. Soc. 71(7), C362 1988
K. Mehta, J.F. Jue A.V. Virkar: Grinding-induced texture in ferroelastic tetragonal zirconia. J. Am. Ceram. Soc. 73(6), 1777 1990
M.V. Swain R.H.J. Hannink: Metastability of the martensitic transformation in a 12 mol% ceria-zirconia alloy: II. Grinding studies. J. Am. Ceram. Soc. 72(8), 1358 1989
C.C. Li, X.W. Zhang Y.J. Xia: The measurement of space distribution of domains in polarized PZT ceramics. Ferroelectrics 37, 623 1981
J.L. Jones, E.B. Slamovich K.J. Bowman: Domain texture distributions in tetragonal lead zirconate titanate by x-ray and neutron diffraction. J. Appl. Phys. 97, 034113 2005
J.L. Jones, E.B. Slamovich K.J. Bowman: Critical evaluation of the lotgering degree of orientation texture indicator. J. Mater. Res. 19(11), 3414 2004
J.L. Jones, S.C. Vogel, E.B. Slamovich K.J. Bowman: Quantifying texture in ferroelectric bismuth titanate ceramics. Scripta Mater. 51, 1123 2004
F.F. Lange, M.R. James D.J. Green: Determination of residual surface stresses caused by grinding in polycrystalline Al2O3. J. Am. Ceram. Soc. 66(2), C16 1983
D. Johnson-Walls, A.G. Evans, D.B. Marshall M.R. James: Residual stresses in machined ceramic surfaces. J. Am. Ceram. Soc. 69(1), 44 1986
J-H. Chen, B-H. Hwang, T-C. Hsu H-Y. Lu: Domain switching of barium titanate ceramics induced by surface grinding. Mater. Chem. Phys. 91, 67 2005
B. Eigenmann E. Macherauch: Determination of inhomogeneous residual stress states in surface layers of machined engineering ceramics by synchrotron x-rays. Nucl. Instrum. Methods in Phys. Res., Sect. B. 97, 92 1995
H. Behnken V. Hauk: Determination of steep stress gradients by x-ray diffraction—Results of a joint investigation. Mater. Sci. Eng., A 300, 41 2000
S.Y. Yu, X.S. Han B. Lin: A study on surface quality of ultraprecision grinding for engineering ceramics. Key Eng. Mater. 202–203, 35 2001
I.A. Cutter R. McPherson: Surface domain reorientation produced by abrasion and annealing of polycrystalline BaTiO3. J. Am. Ceram. Soc. 55(7), 334 1972
A. Yamada, T. Ogawa Y-K. Chung: Crystal orientation of tetragonal lead zirconate titanate ceramic surface and its aging behavior. Jpn. J. Appl. Phys. 36, 5958 1997
M. Hammer, C. Monty, A. Endriss M.J. Hoffmann: Correlation between surface texture and chemical composition in undoped, hard, and soft piezoelectric PZT ceramics. J. Am. Ceram. Soc. 81(3), 721 1998
X. Li, W.Y. Shih, J.S. Vartuli, D.L. Milius, I.A. Aksay W-H. Shih: Effect of a transverse tensile stress on the electric-field-induced domain reorientation in soft PZT: In situ XRD study. J. Am. Ceram. Soc. 85(4), 844 2002
Acknowledgments
This work was supported by the National Science Foundation, DMR-0224991. Materials and assistance were provided by Piezo Technologies, Indianapolis, IN. Thanks also to Elliott Slamovich, William Shelley, and Jacob L. Jones for important discussions and suggestions.
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Chang, W., King, A.H. & Bowman, K.J. Thermal effects on mechanical grinding-induced surface texture in tetragonal piezoelectrics. Journal of Materials Research 22, 2845–2850 (2007). https://doi.org/10.1557/JMR.2007.0355
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DOI: https://doi.org/10.1557/JMR.2007.0355