Abstract
To study the hot deformation behavior of the Ti-22Al-25Nb alloy, isothermal compression tests were conducted at the temperature range of 930–1080 °C with strain rates of 0.001–1.0 s−1. Both the strain rate and the deformation temperature have a significant influence on the stress–strain behavior of the Ti-22Al-25Nb alloy. A hyperbolic–sine constitutive equation is established to quantitatively demonstrate the relationship between the parameters involved, and the hot deformation activation energy Q is determined as 621 kJ/mol. To optimize the processing window, a hot processing map is established, which is related to the microstructure evolution in hot working. The lamellar globularization as well as the dynamic recrystallization (DRX) would contribute to the stable regions with high power dissipation, while the adiabatic shear bands would lead to unstable regions. Moreover, an Avrami-type kinetics model is applied to examine the evolution of DRX during isothermal deformation process.
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References
A.K. Gogia, T.K. Nandy, D. Banerjee, T. Carisey, J.L. Strudel, and J.M. Franchet: Microstructure and mechanical properties of orthorhombic alloys in the Ti-Al-Nb system. Intermetallics 6, 741–748 (1998).
T.K. Nandy and D. Banerjee: Deformation mechanisms in the O phase. Intermetallics 8, 1269–1282 (2000).
S. Emura, K. Tsuzaki, and K. Tsuchiya: Improvement of room temperature ductility for Mo and Fe modified Ti2AlNb alloy. Mater. Sci. Eng., A 528, 355–362 (2010).
L.Q. Xu, D.T. Zhang, Y.C. Liu, B.Q. Ning, Z.X. Qiao, Z.S. Yan, and H.J. Li: Precipitation behavior and martensite lath coarsening during tempering of T/P92 ferritic heat-resistant steel. Int. J. Min. Met. Mater. 21, 438–447 (2014).
S.R. Dey, S. Roy, S. Suwas, J.J. Fundenberger, and R.K. Ray: Annealing response of the intermetallic alloy Ti-22Al-25Nb. Intermetallics 18, 1122–1131 (2010).
S.R. Dey, S. Suwas, J.J. Fundenberger, and R.K. Ray: Evolution of crystallographic texture and microstructure in the orthorhombic phase of a two-phase alloy Ti-22Al-25Nb. Intermetallics 17, 622–633 (2009).
J.B. Jia, K.F. Zhang, and Z. Lu: Dynamic recrystallization kinetics of a powder metallurgy Ti-22Al-25Nb alloy during hot compression. Mater. Sci. Eng., A 607, 630–639 (2014).
C. Xue, W.D. Zeng, B. Xu, X.B. Liang, J.W. Zhang, and S.Q. Li: B2 grain growth and particle pinning effect of Ti-22Al-25Nb orthorhombic intermetallic alloy during heating process. Intermetallics 29, 41–47 (2012).
Y.H. Zhou, Y.C. Liu, X.S. Zhou, C.X. Liu, L.M. Yu, C. Li, and B.Q. Ning: Processing maps and microstructural evolution of the type 347H austenitic heat-resistant stain less steel. J. Mater. Res. 30, 2090–2100 (2015).
X.S. Zhou, C.X. Liu, L.M. Yu, Y.C. Liu, and H.J. Li: Phase transformation behavior and microstructural control of high-Cr martensitic/ferritic heat-resistant steels for power and nuclear plants: A review. J. Mater. Sci. Technol. 31, 235–242 (2015).
Y. Prasad, H. Gegel, S. Doraivelu, J. Malas, J. Morgan, K. Lark, and D. Barker: Modeling of dynamic material behavior in hot deformation: Forging of Ti-6242. Metall. Trans. A 15, 1883–1892 (1984).
D. Samantaray, S. Mandal, and A. Bhaduri: Characterization of deformation instability in modified 9Cr-1Mo steel during thermo-mechanical processing. Mater. Des. 32, 716–722 (2011).
T. Al-Samman and G. Gottstein: Dynamic recrystallization during high temperature deformation of magnesium. Mater. Sci. Eng., A 490, 411–420 (2008).
H.T. Zhou, Q.B. Li, Z.K. Zhao, Z.C. Liu, S.F. Wen, and Q.D. Wang: Hot workability characteristics of magnesium alloy AZ80—A study using processing map. Mater. Sci. Eng., A 527, 2022–2026 (2010).
Y. Xu, L.X. Hu, and Y. Sun: Deformation behaviour and dynamic recrystallization of AZ61 magnesium alloy. J. Alloys Compd. 580, 262–269 (2013).
B.J. Lv, J. Peng, D.W. Shi, A.T. Tang, and F.S. Pan: Constitutive modeling of dynamic recrystallization kinetics and processing maps of Mg-2.0Zn-0.3Zr alloy based on true stress–strain curves. Mater. Sci. Eng., A 560, 727–733 (2013).
A.B. Li, L.J. Huang, Q.Y. Meng, L. Geng, and X.P. Cui: Hot working of Ti-6Al-3Mo-2Zr-0.3Si alloy with lamellar α + β starting structure using processing map. Mater. Des. 30, 1625–1631 (2009).
X. Wang, H. Hamasaki, M. Yamamura, R. Yamauchi, T. Maeda, Y. Shirai, and F. Yoshida: Yield-point phenomena of Ti-20V-4Al-1Sn at 1073K and its constitutive modelling. Mater. Trans. 50, 1576–1578 (2009).
W.J. Jia, W.D. Zeng, Y.G. Zhou, J.R. Liu, and Q.J. Wang: High-temperature deformation behavior of Ti60 titanium alloy. Mater. Sci. Eng., A 528, 4068–4074 (2011).
H. Dehghan, S.M. Abbasi, and A. Momeni: On the constitutive modeling and microstructural evolution of hot compressed A286 iron-base superalloy. J. Alloys Compd. 564, 13–19 (2013).
G.L. Ji, F.G. Li, and Q.H. Li: A comparative study on Arrhenius-type constitutive model and artificial neural network model to predict high-temperature deformation behaviour in Aermet100 steel. Mater. Sci. Eng. A 528, 4774–4782 (2011).
H.J. McQueen and C.A.C. Imbert: Dynamic recrystallization: Plasticity enhancing structural development. J. Alloys Compd. 378, 35–43 (2004).
C.M. Sellars and M.W. Tegart: On the mechanism of hot deformation. Acta Metall. 14(9), 1136–1138 (1966).
G. Meng, B. Li, H. Li, H. Huang, and Z. Nie: Hot deformation and processing maps of an Al–5.7wt%Mg alloy with erbium. Mater. Sci. Eng., A 517, 132–137 (2009).
C. Zener and J.H. Hollomon: Effect of strain rate upon plastic flow of steel. J. Appl. Phys. 15, 22–32 (1944).
S.V.S.N. Murty, M.S. Sarma, and B.N. Rao: On the evaluation of efficiency parameters in processing maps. Metall. Mater. Trans. A 28, 1581–1582 (1997).
C.M. Sellars and W.J.M. Tegart: Hot workability. Int. Metall. Rev. 17, 1–24 (1972).
W. Sha: Crystallization and nematic–isotropic transition activation energies measured using the Kissinger method. J. Appl. Polym. Sci. 80, 2535–2537 (2001).
Y. Sun, W.D. Zeng, Y.Q. Zhao, X.M. Zhang, Y. Shu, and Y.G. Zhou: Research on the hot deformation behavior of Ti40 alloy using processing map. Mater. Sci. Eng., A 528, 1205–1211 (2011).
L. Cheng, H. Chang, B. Tang, H.C. Kou, and J.S. Li: Deformation and dynamic recrystallization behavior of a high Nb containing TiAl alloy. J. Alloys Compd. 552, 363–369 (2013).
A.I. Fernández, P. Uranga, B. López, and J.M. Rodriguez-Ibabe: Dynamic recrystallization behavior covering a wide austenite grain size range in Nb and Nb–Ti microalloyed steels. Mater. Sci. Eng., A 361, 367–376 (2003).
J. Liu, Z. Cui, and L. Ruan: A new kinetics model of dynamic recrystallization for magnesium alloy AZ31B. Mater. Sci. Eng., A 529, 300–310 (2011).
G.L. Ji, F.G. Li, Q.H. Li, H.Q. Li, and Z. Li: Research on the dynamic recrystallization kinetics of Aermet 100 steel. Mater. Sci. Eng., A 527, 2350–2355 (2010).
A. Najafizadeh and J.J. Jonas: Predicting the critical stress for initiation of dynamic recrystallization. ISIJ Int. 46, 1679–1684 (2006).
G.Z. Quan, D.S. Wu, G.C. Luo, Y.F. Xia, J. Zhou, Q. Liu, and L. Gao: Dynamic recrystallization kinetics in α phase of as-cast Ti–6Al–2Zr–1Mo–1V alloy during compression at different temperatures and strain rates. Mater. Sci. Eng., A 589, 23–33 (2014).
ACKNOWLEDGMENTS
The authors are grateful to the China National Funds for Distinguished Young Scientists (granted No. 51325401, and the National Natural Science Foundation of China (Granted No. 51302186)), the National High Technology Research and Development Program of China (Granted No. 2015AA042504) for grant and financial support.
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Zhang, H., Li, H., Guo, Q. et al. Hot deformation behavior of Ti-22Al-25Nb alloy by processing maps and kinetic analysis. Journal of Materials Research 31, 1764–1772 (2016). https://doi.org/10.1557/jmr.2016.188
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DOI: https://doi.org/10.1557/jmr.2016.188