Abstract
Nickel nanoparticles on mass production scale have been prepared using a modified polyol process with Ni(CH3COO)2⋅4H2O, NaOH, 1,2 propandiol and hydrazinium hydroxide (N2H4∗H2O). A mixture of face centered cubic (fcc) metallic nickel nanoparticles with 12 nm diameter were obtained. We have experimentally studied the structure of nanoparticle by X-ray and Scanning Electron Microscopy (SEM, EDS). The magnetic properties of the prepared Ni film have been studied by Ferromagnetic Resonance (FMR) technique, Vibrating Sample Magnetometer (VSM) and Vector Network Analyzer (VNA). The effective g-factor and magnetic anisotropy constant were determined as g eff=2.25 and K eff=85 Oe, respectively.
Similar content being viewed by others
References
Roy, A., Srinivas, V., Ram, S., De Toro, J., Mizutani, U.: Phys. Rev. B 71, 184443 (2005)
Nasongkla, N., Bey, E., Ren, J.M., Ali, H., Khemtong, C., Guthi, J.S., Chin, S.F., Sherry, A.D., Boothman, D.A., Gao, J.M.: Nano Lett. 6, 2427 (2006)
Xu, C.J., Xu, K.M., Gu, H.W., Zheng, R.K., Liu, H., Zhang, X.X., Guo, Z.H., Xu, B.: J. Am. Chem. Soc. 126, 9938 (2004)
Bulte, J.W.M., Douglas, T., Witwer, B., Zhang, S.C., Strable, E., Lewis, B.K., Zywicke, H., Miller, B., Van Gelderen, P., Moskowitz, B.M., Duncan, I.D., Frank, J.A.: Nat. Biotechnol. 19, 1141 (2001)
Lewin, M., Carlesso, N., Tung, C.H., Tang, X.W., Cory, D., Scadden, D.T., Weissleder, R.: Nat. Biotechnol. 18, 410 (2000)
Lee, H., Lee, E., Kim, D.K., Jang, N.K., Jeong, Y.Y., Jon, S.: J. Am. Chem. Soc. 128, 7383 (2006)
Willner, I., Katz, E.: Angew. Chem., Int. Ed. Engl. 42, 4576 (2003)
Mornet, S., Vasseur, S., Grasset, F., Duguet, E.: J. Mater. Chem. 14, 2161 (2004)
Tomita, S., Mitsumata, C.: Phys. Rev. B 71, 180414(R) (2005)
Srajer, G., Lewis, L.H., Bader, S.D., et al.: J. Magn. Magn. Mater. 307, 1 (2006)
Rameev, B.Z., Gupta, A., Miao, G., Xiao, G., Yildiz, F., Tagirov, L.R., Akta, B.: Tech. Phys. Lett. 31(9), 802–805 (2005)
Akdogan, N., Rameev, B.Z., Dorosinsky, et al.: J. Phys., Condens. Matter 17, L359 (2005)
Koseoglu, Y., Yildiz, F., Salazar-Alvarez, G., et al.: Phys. Status Solidi (b). Basic Solid State Phys. 242, 1712 (2005)
Rameev, B.Z., Yildiz, F., Aktas, B., et al.: Microelectron. Eng. 69, 330 (2003)
Yildiz, F., Kazan, S., Aktas, B., et al.: J. Magn. Magn. Mater. 305, 24 (2006)
Rameev, B., Yildiz, F., Kazan, S., et al.: Phys. Status Solidi A 203, 1503 (2006)
Yu, K., Kim, Dong J., Hun, S. Chung, Liang, H.: Mater. Lett. 57, 3992 (2003)
Kartopu, G., Yalcin, O., Kazan, S., et al.: J. Magn. Magn. Mater. 321, 1142 (2009)
Kazan, S., Sale, A.G., Gatiiatova, J.I., et al.: Solid State Commun. 150, 219 (2010)
Stepanov, A.L., Khaibullin, R.I., Rameev, B.Z., Reinholdt, A., Kreibig, U.: Tech. Phys. Lett. 30(2), 151–153 (2004)
Hegde, M.S., Larcher, D., Dupont, L., Budoin, B., Tekaia-Elhsissen, K., Tarascon, J.M.: Solid State Ion. 93, 33 (1997)
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Altınçekiç, T.G., Boz, İ., Basaran, A.C. et al. Synthesis and Characterization of Ferromagnetic Nickel Nanoparticles. J Supercond Nov Magn 25, 2771–2775 (2012). https://doi.org/10.1007/s10948-011-1261-y
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10948-011-1261-y