Abstract
Different techniques for extracting polyaromatic hydrocarbons (PAHs) from coal tar pitch for their quantitative determination by gas chromatography-mass spectrometry are compared. It has been found that the ultrasonic treatment of a sample allowed the quantitative extraction of PAHs from coal tar pitch. The results of the quantitative determination of PAHs in samples of coal tar pitch obtained by Soxhlet extraction and liquid-liquid extraction with ultrasonic treatment agree within the experimental error range.
Similar content being viewed by others
References
Manning, J.A., Burckle, J.O., Hedges, S.R., et al., Determination of Polycyclic Aromatic Hydrocarbons (PAHs) in Ambient Air Using Gas-Chromatography/Mass Spectrometry (GC-MS), Cincinnati: U.S. Environmental Protection Agency, 1999, no. 45268.
Burks, G.A. and Harmon, T.C., J. Chem. Eng. Data, 2001, vol. 46, no. 4, p. 944.
Doick, K.J., Klingelmann, E., Burauel, P., et al., Environ. Sci. Technol., 2005, vol. 39, no. 10, p. 3663.
Becker, G., Colmsjo, A., and Ostman, C., Environ. Sci. Technol., 1999, vol. 33, no. 9, p. 1321.
Lemieux, P., Lutes, C., and Santoianni, D., Progr. Energy Combust. Sci., 2004, vol. 30, p. 1.
Hays, M.D., Smith, N.D., Kinsey, J., et al., J. Aerosol Sci., 2003, vol. 34, no. 8, p. 1061.
Ravindra, K., Godoi, A., Bencs, L., et al., J. Chromatogr., A, 2006, vol. 1114, no. 2, p. 278.
Garcia-Falcon, M.S., Perez-Lamela, M., and Simal-Gandara, J., J. Agric. Food Chem., 2004, vol. 52, no. 23, p. 6897.
Ohe, T., Watanabe, T., and Wakabayashi, K., Mutation Res., 2004, vol. 567, nos. 2–3, p. 109.
King, A.J., Readman, J.W., and Zhou, J.L., Anal. Chim. Acta, 2004, vol. 523, no. 2, p. 259.
Ali, Md.Y. and Cole, R.B., Anal. Chem., 1998, vol. 70, no. 15, p. 3242.
Janska, M., Tomaniov, M., Hajslova, J., et al., Anal. Chim. Acta, 2004, vol. 520, nos. 1–2, p. 93.
Chen, J. and Chen, S., Food Chem., 2005, vol. 90, no. 3, p. 461.
Stolyhwo, A. and Sikorski, Z., Food Chem., 2005, vol. 91, no. 2, p. 303.
Banjoo, D.R. and Nelson, P.K., J. Chromatogr., A, 2005, vol. 1066, nos. 1-2, p. 9.
Bartolome, L., Cortazar, E., Raposo, J.C., et al., J. Chromatogr., A, 2005, vol. 1068, no. 2, p. 229.
Sidorov, O.F. and Seleznev, A.N., Koks Khim., 2006, vol. 50, no. 1, p. 16.
Lesellier, E., Analusis, 1999, vol. 27, no. 4, p. 363.
Morgan, T.J., Millan, M., Behrouzi, M., et al., Energy Fuels, 2005, vol. 19, no. 1, p. 164.
Psillakis, E., Goula, G., Kalogerakis, N., et al., J. Hazard. Mater., B, 2004, vol. 108, nos. 1–2, p. 95.
Little, C., Hepher, M.J., and El-Sharif, M., Ultrasonics, 2002, vol. 40, nos. 1–8, p. 667.
Hassoon, S., Bulatov, V., Yasman, Y., et al., Anal. Chim. Acta, 2004, vol. 512, no. 1, p. 125.
Author information
Authors and Affiliations
Additional information
Original Russian Text © I.M. Afanasov, A.V. Kepman, V.A. Morozov, A.N. Seleznev, V.V. Avdeev, 2009, published in Zhurnal Analiticheskoi Khimii, 2009, Vol. 64, No. 4, pp. 376–381.
Rights and permissions
About this article
Cite this article
Afanasov, I.M., Kepman, A.V., Morozov, V.A. et al. Determination of polyaromatic hydrocarbons in coal tar pitch. J Anal Chem 64, 361–365 (2009). https://doi.org/10.1134/S1061934809040078
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1061934809040078