Abstract
All solvents were purified by distillation before use following standard procedures. Absolute solvents were obtained by distillation over appropriate drying agent (vide infra) and then kept under an atmosphere of argon: diethyl ether, tetrahydrofuran, toluene, and n-hexane (sodium, benzophenone as indicator), chloroform, dichloromethane, triethylamine (calcium hydride), ethanol (magnesium). Absolute 1,4-dioxane, TBME, di(n-butyl)ether, DME, NMP, acetonitrile, and DMSO were purchased from Sigma-Aldrich and used as received. Other commercial reagents were obtained from various sources and used without further purification.
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Notes
- 1.
Relative configuration was assigned on the basis of NOE correlations in collaboration with the NMR department of the Max-Planck-Institut für Kohlenforschung.
References
Ouyang X-Y, Jiang H-F, Huang J-M (2006) Chin J Chem 24:1480
Wynberg H, Marsman B (1980) J Org Chem 45:158
Carlone A, Bartoli G, Bosco M, Pesciaioli F, Ricci P, Sambri L, Melchiorre P (2007) Eur J Org Chem 33:5492
Wang X, Reisinger CM, List B (2008) J Am Chem Soc 130:6070
Rickards RW, Rodwell JL, Schmalzl KJ (1977) J Chem Soc Chem Commun 849
Lv J, Zhang J, Lin Z, Wang Y (2009) Chem Eur J 15:972
Wipf P, Smitrovich JH, Moon CW (1992) J Org Chem 57:3178
Reisinger CM, Wang X, List B (2008) Angew Chem Int Ed 47:8112
Usuda H, Kuramochi A, Kanai M, Shibasaki M (2004) Org Lett 6:4387
Sato T, Kikuchi T, Tsujita H, Kaetsu A, Sootome N, Nishida K-i, Tachibana K, Murayama E (1991) Tetrahedron 47:3281–3304
Scheller ME, Frei B (1992) Helv Chim Acta 75:69
Miyashita M, Suzuki T, Yoshikoshi A (1987) Tetrahedron Lett 28:4293
Dussault PH, Liu X (1999) Org Lett 1:1391
Woods GF, Tucker IW (1948) J Am Chem Soc 70:2174
Woods GF, Griswold PH, Armbrecht BH, Blumenthal DI, Plapinger R (1949) J Am Chem Soc 71:2028
Coote SC, O’Brien P, Whitwood AC (2008) Org Biomol Chem 6:4299
Uyanik M, Fukatsu R, Ishihara K (2009) Org Lett 11:3470
Larock RC, Hightower TR, Kraus GA, Hahn P, Zheng D (1995) Tetrahedron Lett 36:2423
Yu J-Q, Corey EJ (2002) Org Lett 4:2727
Cahiez G, Avedissian H (1998) Synthesis 1199
Zhou J, Wakchaure V, Kraft P, List B (2008) Angew Chem Int Ed 47:7656
Oare DA, Henderson MA, Sanner MA, Heathcock CH (1990) J Org Chem 55:132
Brunner H, Bügler J, Nuber B (1995) Tetrahedron Asymmetry 6:1699
Vakulya B, Varga S, Csámpai A, Soós T (1967) Org Lett 2005:7
Brunner H, Bügler J (1997) Bull Soc Chim Belg 106:77
Franz MH, Röper S, Wartchow R, Hoffmann HMR (2004) J Org Chem 69:2983
Berkessel A, Guixá M, Schmidt F, Neudörfl JM, Lex J (2007) Chem Eur J 13:4483
Chen W, Du W, Duan Y-Z, Wu Y, Yang S-Y, Chen Y-C (2007) Angew Chem Int Ed 46:7667
Kessar SV, Singh P, Singh KN, Singh SK (1999) Chem Commun 19:1927
Lygo B, Crosby J, Lowdon T, Wainwright PG (1999) Tetrahedron 55:2795
Stotter PL, Friedman MD (1985) J Org Chem 50:29
Andrés JM, Manzano R, Pedrosa R (2008) Chem Eur J 14:5116
Martin NJA, Ozores L, List B (2007) J Am Chem Soc 129:8976
Kim KH, Lee S, Lee D-W, Ko D-H, Ha D-C (2005) Tetrahedron Lett 46:5991
Storer RI, Carrera DE, Ni Y, MacMillan DWC (2005) J Am Chem Soc 128:84
Maruoka K, Itoh T, Araki Y, Shirasaka T, Yamamoto H (1988) Bull Chem Soc Jpn 61:2975
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Reisinger, C. (2012). Experimental Part. In: Epoxidations and Hydroperoxidations of α,β-Unsaturated Ketones. Springer Theses. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-28118-1_7
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