Abstract
The thermal treatment of detonation nanodiamonds samples has been performed using synchronous thermal analysis in an argon flow at atmospheric pressure and 600, 800, 1000, 1200, and 1500°C with heating rates of 2 and 10°C/min. X-ray phase analysis of the stored samples shows the thermal stability of some nanodiamond particles up to 1500°C. An electron microscopic investigation of the heat-treated samples shows the effect of the heating rate on the properties of the detonation nanodiamonds powder. Phase changes in detonation nanodiamonds begin in the temperature range of 600–700°C, while the graphitization of diamond nanoparticles synthesized by detonation occurs at temperatures above 800°C.
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Original Russian Text © V.P. Efremov, E.I. Zakatilova, I.V. Maklashova, N.V. Shevchenko, 2018, published in Rossiiskie Nanotekhnologii, 2018, Vol. 13, Nos. 1–2.
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Efremov, V.P., Zakatilova, E.I., Maklashova, I.V. et al. Thermal Analysis of Detonation Nanodiamonds. Nanotechnol Russia 13, 11–17 (2018). https://doi.org/10.1134/S1995078018010044
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DOI: https://doi.org/10.1134/S1995078018010044