Abstract
The crystal structure of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane has been determined by single crystal X-ray diffraction method. The crystal belongs to triclinic system, space group P-1 with unit cell constants a = 11.2877(9) Å, b = 11.9539(9) Å, c = 12.2365(9) Å, α = 97.2580(10)°, β = 116.2850(10)°, γ = 106.3710(10)°, V = 1358.48(18) Å 3, Z = 2, D c = 1.234 g/cm3, μ = 0.079 mm−1, F(000) = 536, R and w(R) are 0.0718 and 0.2055, respectively, for 5239 unique reflections with 3745 observed reflections (I > 2σ(I)).
Similar content being viewed by others
References
Manivannan, G., Gangkakoti, R., Lessard, R. A., Maillot, G., and Bolte, M., J. Phys. Chem. 97, 7228 (1993).
Eaton, D. F., in Advances in Photochemistry, Vol. 13. (Volman, D. H., Hammond, G. S., and Gollnick, K., Editors.), P. 427. Wiley—Interscience, New York, 1986.
Naciri, J. and Weiss, R. G., Macromolecules 22, 3938 (1989).
He, Z., Hammond, G. S., and Weiss, R. G., Macromolecules 25, 502 (1992).
Peres, V. and Nagem, T. J., Phytochemistry 44, 191 (1996).
Peres, V., Nagem, T. J., and de Oliveira, F. F., Phytochemistry 55, 683 (2000).
Ho, C.-K., Huang, Y.-L., and Chen, C.-C., Planta Med. 68, 975 (2002).
Rocha, L., Marston, A., Kaplan, M. A. C., Stoeckli-Evans, H., Thull, U., Testa, B., and Hostettmann, K., Phytochemistry 36, 1381 (1994).
Minami, H., Kinoshita, M., Fukuyama, Y., Kodama, M., Yoshizawa, T., Sugiura, M., Nakagawa, K., and Tago, H., Phytochemistry 36, 501 (1994).
Malet-Cascon, L., Romero, F., Espliego-Vazquez, F., Gravalos, D., and Fernandez-Puentes, J. L., J. Antibiot. 56, 219 (2003).
Lin, C. N., Chung, M. I., Liou, S. J., Lee, T. H., and Wang, J. P., J. Pharm. Pharmacol. 48, 532 (1996).
Groweiss, A., Cardellina II, J. H., and Boyd, M. R., J. Nat. Prod. 63, 1537 (2000).
Zhou, W. H., Liu, J. M., Li, M. Z., and Wang, E. J., Dyes Pigments 36, 295 (1998).
Zhou, W. H., Liu, J. M., Wu, Z. R., and Wang, E. J., J. Photochem. Photobiol., A 112, 173 (1998).
Panunzi, A., Giordano, F., Orabona, I., and Ruffo, F., Inorg. Chim. Acta 358, 1217 (2005).
Sheldrick, G. M., SHELXS-97, Program for X-Ray Crystal Structure Solution. Göttingen University, Germany, 1997; Sheldrick, G. M., SHELXS-97, Program for X-Ray Crystal Structure Refinement. Göttingen University, Germany, 1997.
Allen, F. H., Kennard, O., Watson, D. G., Brammer, L., Orpen, A. G., and Taylor, R., J. Chem. Soc., Perkin Trans. 2 1987, S1.
Ding, C.-F., Tian, B.-Q., Li, X.-M., Liu, Q., Zhang, S.-S., Xu, H., and Ouyang, P.-K., Asian J. Chem. 18, 1430 (2006).
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Li, X.M., Ding, C.F., Tian, B.Q. et al. Crystal structure and thermal chemical properties of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane. Chem. Pap. 60, 220–223 (2006). https://doi.org/10.2478/s11696-006-0039-3
Received:
Revised:
Accepted:
Issue Date:
DOI: https://doi.org/10.2478/s11696-006-0039-3