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High-Resolution Solid-State NMR

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NMR in Biological Systems

Part of the book series: Focus on Structural Biology ((FOSB,volume 6))

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References

6.1 Further Reading

  • E.R. Andrew, A. Bradbury, A. and R.G. Eades, Removal of dipolar broadening of nuclear magnetic resonance spectra of solids by specimen rotation, Nature 183, 1802–1803 (1959).

    Article  CAS  Google Scholar 

  • I.J. Lowe, Free induction decays of rotating solids, Phys. Rev. Lett. 2, 285–287 (1959).

    Article  CAS  Google Scholar 

  • A. Pines, M.G. Gibby, and J.S. Waugh, Proton-enhanced NMR of dilute spins in solids, J. Chem. Phys. 59, 569–590 (1973).

    Article  CAS  Google Scholar 

  • A. Seelig, and J. Seelig, Effect of a local anaesthetic on hydrocarbon chain order in membranes Biochemistry 13, 4839–4845 (1974).

    Article  CAS  Google Scholar 

  • J. Schaefer, and E.O. Stejskal, Carbon-13 nuclear magnetic resonance of polymers spinning at the magic angle, J. Am. Chem. Soc. 98, 1031–1032 (1976).

    Article  CAS  Google Scholar 

  • A.H. Roufosse, W.P. Aue, J.E. Roberts, M.J. Glimcher, and R.G. Griffin, Investigation of mineral phases of bone by solid-state phosphorus-31 magic angle spinning nuclear magnetic resonance, Biochemistry 23, 6115–6120 (1984).

    Article  CAS  Google Scholar 

  • R.L. Smith, and E. Oldfield, Dynamic structure of membranes by deuterium NMR, Science 225, 280–287 (1984).

    Article  CAS  Google Scholar 

  • F.M. Marassi and S.J. Opella, NMR structural studies of membrane proteins, Curr. Opin. Struc. Biol. 8, 640–648 (1998).

    Article  CAS  Google Scholar 

  • F.M. Marassi, and S.J. Opella, A solid-state NMR index of helical membrane protein structure and topology, J. Mag. Res. 144, 150–155 (2000).

    Article  CAS  Google Scholar 

  • J. Pauli, B. Rossum, H. Forster, H.J.M. Groot, and H. Oschkinat, Sample optimization and identification of signal patterns of amino acid side chains in 2D RFDR spectra of the α -spectrin SH3 domain, J. Mag. Res. 143, 411–416 (2000).

    Article  CAS  Google Scholar 

  • F. Castellani, B. van Rossum, A. Diehl, M. Schubert, K. Rehbein and H. Oschkinat, Structure of a protein determined by solid-state magic-angle-spinning NMR spectroscopy, Nature 420, 98–102 (2002).

    Article  CAS  Google Scholar 

  • D.D. Laws, H.L. Bitter, and A. Jerschow, Solid-State NMR Spectroscopic Methods in Chemistry, Angew. Chem. Int. Ed. 41, 3096–3129 (2002).

    Article  CAS  Google Scholar 

  • B.J. Van Rossum, E.A.M. Schulten, J. Raap, H. Oschkinat, and H.J.M. Groot, A 3-D structural model of self assembled chlorophyll a/H 2 O from multispin labeling and MAS NMR 2-D dipolar correlation spectroscopy in high magnetic field,J. Mag. Res. 155, 1–14 (2002).

    Article  CAS  Google Scholar 

  • B. Bechinger, and C. Sizun, Alignment and structural analysis of membrane polypeptides by 15 N and 31 P solid-state NMR spectroscopy, Concepts Magn. Reson. 18A, 130–145 (2003).

    Article  CAS  Google Scholar 

  • S. Luca, H. Heise, and M. Baldus, High-resolution solid-state NMR: Applied to Polypeptides and membrane proteins, Acc. Chem. Res. 36, 858–865 (2003).

    Article  CAS  Google Scholar 

  • P.T. Eles and C.A. Michal, A DECODOR NMR study of backbone orientation in Nephila clavipes dragline silk under varying strain and draw rate, Biomacromolecules 5, 661–665 (2004).

    Article  CAS  Google Scholar 

  • A. Simmons, S.K. Sarkar, and L.W. Jelinski, Solid-state NMR and Its Applications to Biological Research,inNMR Spectroscopy and Its Application to Biomedical Research, S.K. Sarkar (ed.) \newline pp. 345–380 (1996).

    Google Scholar 

  • T.I. Igumenova, A.E. McDermott, K. Zim, R.W. Martin, E.K. Paulson, and A.J. Wand, Assignments of carbon resonances for microcrystalline ubiquitin,J. Am. Chem. Soc. 126, 6720–6727 (2004).

    Article  CAS  Google Scholar 

  • B. Brodsky and A.V. Persikov, Molecular structure of the collagen triple helix, Adv. Protein Chem. 70,301–338 (2005).

    Article  CAS  Google Scholar 

  • D. Huster, Investigations of the structure and dynamics of membrane-associated peptides by magic angle spinning NMR, Prog. Nucl. Magn. Reson. Spectrosc. 46, 79–107 (2005).

    CAS  Google Scholar 

  • R. Tycko, Molecular structure of amyloid fibril: insights from solid-state NMR, Q. Rev. Biophys. 39, 1–55 (2006).

    Article  CAS  Google Scholar 

6.2 Books and Reviews

  • C.A. Fyfe, Solid-State NMR for Chemists, C.F.C. Press, Guelph, Canada (1983).

    Google Scholar 

  • K. Schmidt-Rohr, and H.W. Speiss, Multidimensional Solid NMR and Polymers,Academic Press (1994).

    Google Scholar 

  • M.H. Levitt., Spin Dynamics. Basics of Nuclear Magnetic Resonance, John Wiley & Sons., Singapore (2001).

    Google Scholar 

  • M.J. Duer (ed.), Solid-state NMR Spectroscopy: Principles and Applications, Blackwell Science (2002).

    Google Scholar 

  • A.S. Ulrich, and A. Ramammorthy (eds), Solid-state NMR on biological systems(Special Issue), Mag. Res. Chem. 42(2), (2004).

    Article  CAS  Google Scholar 

  • H. Saito, I. Ando and A. Naito, Solid-State NMR for Biopolymers: Principles and Applications, Springer (2006).

    Google Scholar 

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Chary, K., Govil, G. (2008). High-Resolution Solid-State NMR. In: Chary, K., Govil, G. (eds) NMR in Biological Systems. Focus on Structural Biology, vol 6. Springer, Dordrecht. https://doi.org/10.1007/978-1-4020-6680-1_9

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