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Apparatus

Preliminary Comments

  • Chapter
Gas Phase Chromatography
  • 164 Accesses

Abstract

All chromatographic methods require apparatus. But while a developed paper chromatogram is in existence for a given time, in a gas chromatogram everything is continually changing, and it is necessary at the first stage of separation to carry out the ‘development’ and the preliminary evaluation of the chromatogram at one and the same time. Special instruments are needed to record the separated substances, because, generally speaking, in gas chromatography these cannot be made visible, as in paper chromatography, or weighed after removal of the liquid phase, as in column chromatography. It is therefore important to record the chromatographic result at once. As a gas chromatogram results from the fact that the individual components, starting at a given time, move through the column at different speeds, it is necessary to measure not only the quantity of substance but also the time at which it leaves the column. It has been said that the classical methods of obtaining a chromatogram by making the components visible or by weighing them can generally not be used in the case of gas chromatography. The difference between gas chromatography and the other chromatographic processes with respect to the apparatus needed may be made clear from the example of the flame emission process, which will be described in more detail in the section on detectors.

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© 1960 Bibliographisches Institut AG Mannheim

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Kaiser, R. (1960). Apparatus. In: Gas Phase Chromatography. Springer, Boston, MA. https://doi.org/10.1007/978-1-4684-8291-1_3

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