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Apparatus for the Accurate Measurements of Magnetic Susceptibility with the Help of a Vacuum Electrobalance

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Vacuum Microbalance Techniques

Abstract

Best conditions for magnetic susceptibility measurements of diamagnetic or slightly paramagnetic fluids are stated. It is pointed out that the classical Gouy method is the most favorable.

A simple apparatus consisting essentially of a slightly modified Cahn RH Electrobalance, a permanent magnet, and thermostatic devices, is described. This apparatus can operate under high vacuum or in controlled gas atmosphere from −30 to 150 C with an accuracy about 2 × 10−10 emu even on samples with a total weight greater than 50–60 g. Operating procedures are discussed to minimize experimental errors. The apparatus was used for a new determination of magnetic susceptibility temperature coefficient of water over the temperature range 0–80 C; a comparison between the results obtained and the existing data is reported. Finally, the use of this apparatus is suggested for simultaneous adsorption and magnetic-susceptibility change measurements on powders which possess no paramagnetism.

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© 1970 Plenum Press, New York

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Cini, R., Torrini, M. (1970). Apparatus for the Accurate Measurements of Magnetic Susceptibility with the Help of a Vacuum Electrobalance. In: Massen, C.H., van Beckum, H.J. (eds) Vacuum Microbalance Techniques. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-0725-0_5

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  • DOI: https://doi.org/10.1007/978-1-4757-0725-0_5

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4757-0727-4

  • Online ISBN: 978-1-4757-0725-0

  • eBook Packages: Springer Book Archive

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