Abstract
A solution of 57.3 g (0.3 mole) of 5-bromo-2-furoic acid (see Vol. 1 of this work, p. 11),m.p. 182–183°, in 150 ml of dry benzene was prepared in a 300-ml round-bottomed flask fitted with reflux condenser protected by a calcium chloride tube, and 42.8 g (0.36 mole) of freshly distilled thionyl chloride was added.
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Literature Cited
L. C. Raiford and W. G. Huey, J. Org. Chem. 6, 858 (1941)
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A. L. Mndzhoian, Zh. obshchei khim. (J. Gen. Chem.) 16, 751 (1946).
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Mndzhoian, A.L. (1959). 5-Bromo-2-Furoyl Chloride. In: Mndzhoian, A.L. (eds) Syntheses of Heterocyclic Compounds. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-6658-5_57
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DOI: https://doi.org/10.1007/978-1-4757-6658-5_57
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