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Influence of Calcination Temperatures on the Morphology and Specific Surface Area Development of ZrO2-CeO2-Y2O3-Al2O3 Powders Obtained via Sol-Gel Route

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Innovations in Biomedical Engineering (IBE 2017)

Part of the book series: Advances in Intelligent Systems and Computing ((AISC,volume 623 ))

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Abstract

BACKGROUND: Doped with metal oxide, zirconia is one of the most currently used ceramics for making a wide range of all-ceramic restorations in dental prosthetics. Its use entails very good mechanical properties and the possibility of obtaining a desirable aesthetic effect of manufactured prostheses.

OBJECTIVE: The main purpose/aim of this study was to investigate the influence of calcination temperature on the morphology and specific surface area development of a ZrO2 – CeO2 – Y2O3 – Al2O3 powder system obtained with a humidfree sol-gel process.

METHODS: Powders were obtained by the sol-gel method in an inert gas atmosphere at ambient temperature using, for this purpose, zirconium n-propoxide. Morphology was examined by scanning electron microscopy (SEM), and specific surface area was investigated with full-adsorption isotherms in nitrogen with a Brunauer-Emmett-Teller model (BET).

RESULTS: Depending on the calcination temperature, different morphologies and surface areas were observed.With an increase in temperature, grain growth was observed.

CONCLUSIONS: The influence of calcination temperature on morphology and specific surface area of the as-obtained powders was clearly evidenced.

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Author information

Authors and Affiliations

  1. Department of Biomaterials and Medical Devices Engineering, Faculty of Biomedical Engineering, Silesian University of Technology, Roosevelta 40 st., 41-800, Zabrze, Poland

    Damian S. Nakonieczny, Zbigniew K. Paszenda, Magdalena Antonowicz & Agata Sambok

  2. Department of Biosensors and Biomedical Signal Processing, Faculty of Biomedical Engineering, Silesian University of Technology, Roosevelt 40 st., 41-800, Zabrze, Poland

    Justyna Majewska

  3. Department of Optoelectronics, Silesian University of Technology, B. Krzywoustego 2 st., Gliwice, Poland

    Sabina Drewniak

  4. Department of Chemical Engineering and Process Design, Faculty of Chemistry, Silesian University of Technology, M. Strzody 7 st., Gliwice, Poland

    Wojciech Bogacz

  5. Department of Dental Technology, Medical College of Zabrze, 3 maja 63 st., Zabrze, Poland

    Cezary Krawczyk

Authors
  1. Damian S. Nakonieczny
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  2. Zbigniew K. Paszenda
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  3. Justyna Majewska
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  4. Sabina Drewniak
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  5. Wojciech Bogacz
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  6. Magdalena Antonowicz
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  7. Agata Sambok
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  8. Cezary Krawczyk
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Corresponding author

Correspondence to Damian S. Nakonieczny .

Editor information

Editors and Affiliations

  1. Department of Biomechatronics, Silesian University of Technology, Faculty of Biomedical Engineering, Zabrze, Poland

    Marek Gzik

  2. Department of Biosensors and Biomedical Signals Processing, Silesian University of Technology, Faculty of Biomedical Engineering, Zabrze, Poland

    Ewaryst Tkacz

  3. Department of Biomaterials and Medical Devices Engineering, Silesian University of Technology, Faculty of Biomedical Engineering, Zabrze, Poland

    Zbigniew Paszenda

  4. Dept. of Informatics and Medical Equipment, Silesian University of Technology, Faculty of Biomedical Engineering, Zabrze, Poland

    Ewa Piętka

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Nakonieczny, D.S. et al. (2018). Influence of Calcination Temperatures on the Morphology and Specific Surface Area Development of ZrO2-CeO2-Y2O3-Al2O3 Powders Obtained via Sol-Gel Route. In: Gzik, M., Tkacz, E., Paszenda, Z., Piętka, E. (eds) Innovations in Biomedical Engineering . IBE 2017. Advances in Intelligent Systems and Computing, vol 623 . Springer, Cham. https://doi.org/10.1007/978-3-319-70063-2_38

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  • DOI: https://doi.org/10.1007/978-3-319-70063-2_38

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  • Publisher Name: Springer, Cham

  • Print ISBN: 978-3-319-70062-5

  • Online ISBN: 978-3-319-70063-2

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