Abstract
In this paper, we propose an advanced approach to particle analysis, involving laser-induced breakdown spectroscopy (LIBS) and laser-induced incandescence (LII) temporal analytical techniques. Various technical properties of fine particles are analyzed via LIBS and LII. LIBS is a useful tool for determining the elemental composition and relative concentration of various materials, whereas LII facilitates the measurement of particle size. Both techniques do not require any pre-processing. The combined use of the LIBS and LII techniques enables highly synergistic fine particle measurement. In the LIBS section, we propose spectrometric analysis via a novel ink-jet technique, and we discuss the effectiveness of Ar as a surrounding gas. In the LII section, we compare the calculated particle size prediction with the experimental results.
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References
Andreev, A., Ueda, T.: Simulation of laser plasma emission characteristics of small solid particles in different gas atmospheres at various pressures. Trans. IEE of Japan 121-E(11), 593–598 (2001)
Wakamatsu, M., Ikezawa, S., Ueda, T.: Particle element and size simultaneous measurement using LIBS. IEEJ Transactions on Sensors and Micromachines 127(9), 397–402 (2007)
Ikezawa, S., Wakamatsu, M., Pawlat, J., Ueda, T.: Sensing System for Multiple Measurements of Trace Elements Using Laser-induced Breakdown Spectroscopy. IEEJ Transactions on Sensors and Micromachines 129(4), 115–119 (2009)
Brown, J.H., Cook, K.M., Ney, F.G., Hatch, T.: Influence of Particle Size upon the Retention of Particulate Matter in the Human Lung. American Journal of Public Health Nations Health, 450–458 (1950)
Kodavanti, U.P., Schladweiler, M.C., Ledbetter, A.D., Watkinson, W.P., Campen, M.J., Winsett, D.W., Richards, J.R., Crissman, K.M., Hatch, G.E., Costa, D.L.: The Spontaneously Hypertensive Rat as a Model of Human Cardiovascular Disease: Evidence of Exacerbated Cardiopulmonary Injury and Oxidative Stress from Inhaled Emission Particulate Matter. Toxicology and Applied Pharmacology 164(3), 250–263 (2000)
Squadrito, G.L., Rafael, C., Dellinger, B., Pryor, W.A.: Quinoid redox cycling as a mechanism for sustained free radical generation by inhaled airborne particulate matter. Free Radical Biology and Medicine 31(9), 1132–1138 (2001)
Carll, A.P., Haykal-Coates, N., Winsett, D.W., Rowan III, W.H., Hazari, M.S., Ledbetter, A.D., Nyska, A., Cascio, W.E., Watkinson, W.P., Costa, D.L., Farraj, A.K.: Particulate matter inhalation exacerbates cardiopulmonary injury in a rat model of isoproterenol-induced cardiomyopathy. Inhalation Toxicology, 1–14 (2010)
Eckbreth, A.C.: Effects of Laser-Modulated Particulate Incandescence on Raman Scattering Diagnostics. Journal of Applied Physics 48, 4473–4479 (1977)
Melton, L.A.: Soot Diagnostics Based on Laser Heating. Applied Optics 23, 2201–2208 (1984)
Jenkins, T.P., Bartholomew, J.L., DeBarber, P.A., Yang, P., Seitzman, J.M., Howard, R.P.: Laser Induced Incandescence for Soot Concentration Measurements in Turbine Engine Exhausts. In: AIAA paper 2002-0828 (2002)
Michelsen, H.A.: Understanding and Predicting the Temporal Response of Laser-induced Incandescence from Carbonaceous Particles. Journal of Chemical Physics 118, 7012–7045 (2003)
McCoy, B.J., Cha, C.Y.: Transport phenomena in the rarefied gas transition regime. Chemical Engineering Science 29(2), 381–388 (1974)
Wu, C.H., Mszanowski, U., Martin, J.M.L.: The impact of larger clusters formation C5, C6, C7, C8, C9, and C10 on the rates of carbon sublimation at elevated temperatures. Journal of Nuclear Materials 258-263(Part 1), 782–786 (1998)
Arepalli, S., Scott, C.D., Nikolaev, P., Smalley, R.E.: Electronically excited C2 from laser photodissociated C60. Chemical Physics Letters 320(1-2), 26–34 (2000)
Vietzke, E., Refke, A., Philipps, V., Hennes, M.: Energy distributions and yields of sputtered C2 and C3 clusters. Journal of Nuclear Materials 241-243, 810–815 (1997)
Philipps, V., Vietzke, E., Flaskamp, K.: Sticking probabilities of evaporated C1, C2 and C3 on pyrolytic graphite. Surface Science 178(1-3), 806–812 (1986)
Brewer, L., Kane, J.S.: The Importance of Complex Gaseous Molecules in High Temperature Systems. The Journal of Physical Chemistry 59(2), 105–109 (1955)
Bukatyi, V.I., Zhdanov, E.P., Shaiduk, A.M.: Combustion of aerosol particles in an electromagnetic field. Combustion, Explosion, and Shock Waves 18(3), 309–312 (1982)
Konno, T.J., Sinclair, R.: Crystallization of amorphous carbon in carbon—cobalt layered thin films. Acta Metallurgica et Materialia 43(2), 471–484 (1995)
Marcos, P.A., López, M.J., Rubio, A., Alonso, J.A.: Thermal road for fullerene annealing. Chemical Physics Letters 273(5-6), 367–370 (1997)
Samsonidze, G.G., Samsonidze, G.G., Yakobson, B.I.: Kinetic Theory of Symmetry-Dependent Strength in Carbon Nanotubes. Physical Review Letters 88(6), (065501-1) – (065501-4) (2002)
Banhart, F., Füller, T., Redlich, P., Ajayan, P.M.: The formation, annealing and self-compression of carbon onions under electron irradiation. Chemical Physics Letters 269(3-4), 349–355 (1997)
Wang, B.-C., Wang, H.-W., Chang, J.-C., Tso, H.-C., Chou, Y.-M.: More spherical large fullerenes and multi-layer fullerene cages. Journal of Molecular Structure: THEOCHEM 540(1-3), 171–176 (2001)
Atamny, F., Bloecker, J., Henschke, B., Schloegl, R., Schedel-Niedrig, T., Keil, M., Bradshaw, A.M.: Reaction of oxygen with graphite: x-ray absorption spectroscopy of carbonaceous materials. The Journal of Physical Chemistry 96, 4522–4526 (1992)
Fried, L.E., Howard, W.M.: Explicit Gibbs free energy equation of state applied to the carbon phase diagram. Physical Review B 61(13), 8734–8743 (2000)
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Ikezawa, S., Wakamatsu, M., Zimin, Y.L., Pawlat, J., Ueda, T. (2011). Multi-spectral Analytical Systems Using LIBS and LII Techniques. In: Mukhopadhyay, S.C., Lay-Ekuakille, A., Fuchs, A. (eds) New Developments and Applications in Sensing Technology. Lecture Notes in Electrical Engineering, vol 83. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-17943-3_11
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DOI: https://doi.org/10.1007/978-3-642-17943-3_11
Publisher Name: Springer, Berlin, Heidelberg
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