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Study of Submicrocrystalline Materials by Diffuse Scattering in Transmitted Wave

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Diffraction Analysis of the Microstructure of Materials

Part of the book series: Springer Series in Materials Science ((SSMATERIALS,volume 68))

Abstract

A new method of crystallite size determination has been applied to submicrocrystalline materials prepared by high-pressure torsion deformation. The method is based on the measurement of the small-angle diffuse scattering in the transmitted wave and requires thin foil samples and well-defined incoming plane wave. The physical information is encoded in the wave modification due to primary extinction in the crystallites.

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References

  1. J. Cízek, I. Procházka, R. Kužel, R.K. Islamgaliev: Monatshefte für Chemie, Vol. 133, No. 6, pp. 873–887, (2002)

    Article  Google Scholar 

  2. R. Kuzel, J. Čízek, I. Procházka, F. Chmelík, R.K. Islamgaliev, N.M. Amirkhanov: Materials Science Forum 378–381 (2), 463 (2001)

    Article  Google Scholar 

  3. J. Cízek, I. Procházka, O. Melikhova, G. Brauer, W. Anwand, R. Kuzel, M. Cieslar, R.K. Islamgaliev: Applied Surface Science, Vol. 194, No. 1–4, pp. 140–144, (2002)

    Article  Google Scholar 

  4. J. Cízek, I. Procházka, M. Cieslar, R. Kuzel, J. Kuriplach, F. Chmelík, I. Stulíková, F. Bečvář, O. Melikhova, R.K. Islamgaliev: Phys. Rev. B 65, 094–106 (2002)

    Article  Google Scholar 

  5. M. Cerňanský, V. Holý, J. Kub, J. Kubena: Materials Structure. Vol. 5, Special Issue B, (1998) p. 201 and to be published

    Google Scholar 

  6. B.E. Warren: X-ray diffraction. (Reading, Massachusetts. 1969)

    Google Scholar 

  7. H.P. Klug, L.E. Alexander: X-ray diffraction procedures for polycrystalline and amorphous materials. (John Wiley and Sons, New York 1974)

    Google Scholar 

  8. M.A. Krivoglaz: X-ray and neutron diffraction in nonideal crystals. (Springer, Berlin Heidelberg New York 1996)

    Google Scholar 

  9. Defect and Microstructure Analysis by Diffraction. Eds. R. Snyder, J. Fiala and H. Bunge (Oxford University Press 1999)

    Google Scholar 

  10. D. Breuer, P. Klimanek, W. Pantleon: J. Appl. Cryst. 33, 1284 (2000)

    Article  Google Scholar 

  11. T. Ungár, I. Dragomir, A. Révész, A. Borbély: J. Appl. Cryst. 32, 992 (1999)

    Article  Google Scholar 

  12. T. Ungár, J. Gubicza, G. Ribárik, A. Borbély: J. Appl. Cryst. 34, 298 (2001)

    Article  Google Scholar 

  13. G. Ribárik, T. Ungár, J. Gubicza: J. Appl. Cryst. 34, 298 (2001)

    Article  Google Scholar 

  14. P. Scardi, M. Leoni: Acta Crystallographica, A 58, 190 (2002)

    Google Scholar 

  15. P. Scardi, M. Leoni, Y.H. Dong: Eur. Phys. J. B 18, 23 (2000)

    Article  ADS  Google Scholar 

  16. A. Guinier, G. Fournet: Small-angle scattering of X-rays. (John Wiley, New York 1955)

    Google Scholar 

  17. Small angle X-ray scattering. Ed. O. Glatter and O. Kratky (Academic Press, London 1982)

    Google Scholar 

  18. M. Born and E. Wolf: Principles of Optics: Electromagnetic Theory of Propagation, Interference and Diffraction of Light. 7th edn (Cambridge University Press, Cambridge 1999)

    Google Scholar 

  19. L.V. Azaroff, R. Kaplow, N. Kato, R.J. Weiss, A.J.C. Wilson, and R.A. Young: X-Ray Diffraction (McGraw-Hill, New York 1974)

    Google Scholar 

  20. R.Z. Valiev: Mat. Sci. Eng. A 234–236, 59 (1998)

    Google Scholar 

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© 2004 Springer-Verlag Berlin Heidelberg

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Kužel, R., Holý, V., Čerňanský, M., Kubéna, J., Šimek, D., Kub, J. (2004). Study of Submicrocrystalline Materials by Diffuse Scattering in Transmitted Wave. In: Mittemeijer, E.J., Scardi, P. (eds) Diffraction Analysis of the Microstructure of Materials. Springer Series in Materials Science, vol 68. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-06723-9_9

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  • DOI: https://doi.org/10.1007/978-3-662-06723-9_9

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-642-07352-6

  • Online ISBN: 978-3-662-06723-9

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