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Study of the Correlations Between the Dynamics of Thermal Destruction and the Morphological Parameters of Biogenic Calcites by the Method of Thermoprogrammed Desorption Mass Spectrometry (TPD-MS)

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Microstructure and Properties of Micro- and Nanoscale Materials, Films, and Coatings (NAP 2019)

Part of the book series: Springer Proceedings in Physics ((SPPHY,volume 240))

Abstract

By the method of thermoprogrammed mass spectrometry (TPD-MS) were studied the biogenic calcites thermal desorption spectra (natural limestone chalk, bird eggshells: chicken (Gallus gallus domesticus), domestic turkey (Meleagris gallopavo), domestic geese (Anser anser domesticus), domestic duck (Cairina moschata), mollusk shells (Anadara inaequivalvis), and cephalopod fossils Belemnite (Pachyteuthis Bayle), as well as calcite nanoparticles. It was shown that the structure of the spectrum correlates with morphological parameters and is a function of samples dispersity degree of biogenic calcites. The increase in the content of nano-, ultra- and microdispersed components in calcite-based biocomposites leads to a significant change in the form of the thermal desorption spectrum, manifested in the appearance of additional temperature desorption areas (peaks) in thermograms and their displacement to lower temperatures area.

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Acknowledgements

The work has been performed under the financial support of the Ministry of Education and Science of Ukraine (Introduction of nanocomposite materials in innovative technologies for the incubation of poultry eggs; state registration number 0119U100551).

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Authors and Affiliations

  1. Sumy National Agrarian University, 160, Herasym Kondratiev Str., Sumy, 40021, Ukraine

    O. G. Bordunova, V. B. Loboda, Y. A. Samokhina & R. V. Dolbanosova

  2. Dnipro State Agrarian and Economic University, 25, S. Efremov St., Dnipro, 49600, Ukraine

    O. M. Chernenko

  3. Institute of Applied Physics (IAP), NAS of Ukraine, 58, Petropavlovskaya Str., Sumy, 40001, Ukraine

    V. D. Chivanov

Authors
  1. O. G. Bordunova
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  2. V. B. Loboda
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  3. Y. A. Samokhina
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  4. O. M. Chernenko
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  5. R. V. Dolbanosova
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  6. V. D. Chivanov
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Corresponding author

Correspondence to O. G. Bordunova .

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Editors and Affiliations

  1. Sumy State University, Sumy, Ukraine

    Alexander D. Pogrebnjak

  2. Sumy State University, Sumy, Ukraine

    Oleksandr Bondar

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Bordunova, O.G., Loboda, V.B., Samokhina, Y.A., Chernenko, O.M., Dolbanosova, R.V., Chivanov, V.D. (2020). Study of the Correlations Between the Dynamics of Thermal Destruction and the Morphological Parameters of Biogenic Calcites by the Method of Thermoprogrammed Desorption Mass Spectrometry (TPD-MS). In: Pogrebnjak, A., Bondar, O. (eds) Microstructure and Properties of Micro- and Nanoscale Materials, Films, and Coatings (NAP 2019). Springer Proceedings in Physics, vol 240. Springer, Singapore. https://doi.org/10.1007/978-981-15-1742-6_5

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